CAUTION

Gas Filter Rupture upon Excessive Gas Supply Pressure

An excessive supply gas pressure can lead to an overpressure in the detector and can cause the gas filters to rupture. This can pose a health and safety risk.

  • Turn on the gas supply only when the gas filters are properly connected to the detector and the protective cover is properly installed.
  • Observe the gas supply pressure range that is specified for the detector. Do not exceed the maximum gas supply pressure.
  • Before you start the replacement of the gas filter assembly, make sure that the gas supply and the detector gas flow are turned off.
  • Observe the gas supply requirements. See Gas Supply Requirements.

CAUTION

Escaping Gas

Gas can escape from open gas connections when the detector gas flow and/or the gas supply is turned on. The escaping gas can pose a health and safety risk.

  • Make sure that the detector gas flow and the gas supply are turned off before you remove the nebulizer, disconnect the gas tubes or remove the gas filter assembly from the detector.
  • Turn on the gas supply and detector gas flow only when the nebulizer is installed, the components in the gas flow path are properly connected, and the protective cover of the gas filter assembly is installed.

When

Interval for gas filter replacement has expired

Parts required

Gas filter assembly consisting of a charcoal gas filter and a HEPA gas filter

Tools required

Screwdriver, Torx T10

Preparations

  1. Flush the detector with the detector gas flow being turned on. For recommendations on flushing the detector, see Flushing the Detector Between Analyses.

  1. Turn off the pump flow and then the gas flow:

  1. Turn off the pump flow to the detector. Wait at least 5 minutes. During the waiting period, the detector drains any remaining mobile phase to waste.
  2. Turn off the gas flow on the detector.
  3. Wait until the system pressure is down to zero before you continue.
  4. Turn off the gas supply to the detector.
  1. Turn off the detector with the main power switch.

Follow these steps

  1. With the screwdriver, loosen and remove the top screw on the protective cover for the gas filter assembly.

  2. Gas filter assembly with protective cover
    Figure: Gas filter assembly with protective cover

    No.

    Description

    1

    Top screw on protective cover

    2

    Protective cover

    3

    Bottom screws (slightly loosened)

    4

    Gas filters

  3. Slightly loosen the two bottom screws on the protective cover. Leave the two screws attached loosely in the bores. Do not remove the screws.

  4. Push the protective cover upward to release it from the two bottom screws (no. 1 in the image below). Lift the protective cover away from the front panel (no. 2 in the image below).

Removing the protective cover
Figure: Removing the protective cover

The gas filters are uncovered now:

Gas filter assembly
Figure: Gas filter assembly

No.

Description

1

Charcoal gas filter

2

Elbow fittings

3

HEPA gas filter

4

Gas filter clamps

  1. Disconnect the gas filter assembly from the gas connectors on the detector:

  1. On the two (push-in) elbow fittings on the detector gas connectors, push in the locking ring on each elbow fitting (no. 1 in the image below) and keep pushing it while performing the next step.
    Leave the elbow fittings connected to the gas filter assembly.
  2. Pull the two elbow fittings off from the gas connectors on the detector (no. 2 in the image below).
Unlocking an elbow fitting
Figure: Unlocking an elbow fitting
  1. Pull the gas filter assembly out of the clamps.

  2. Pulling the gas filter assembly out of the clamps
    Figure: Pulling the gas filter assembly out of the clamps
  3. With the new gas filter assembly, mind the correct orientation for the gas flow for installation. Observe the flow direction signs on the filters.

    • The bottom gas filter must be the charcoal gas filter (thick black inner filter cylinder; no. 2 in the image below).

    • The top gas filter must be the HEPA gas filter (thin white inner filter cylinder; no. 1 in the image below).

  4. Push the new gas filter assembly into the clamps observing the orientation signs for the gas flow on the gas filters. See image below.

  5. Correct orientation of the gas filter assembly
    Figure: Correct orientation of the gas filter assembly

    No.

    Description

    1

    HEPA gas filter

    2

    Charcoal gas filter

  6. Push the (push-in) elbow fittings into the gas connectors on the detector. Check that the connections are secure: Slightly pull on the fittings. If a fitting slides out, repeat this step.

  7. Install the protective cover: Hold the protective cover onto the interior panel. Slide it downward carefully so that the bottom screws match the recesses.

  8. With the screwdriver, tighten the three screws on the protective cover.

  9. Turn on the detector with its main power switch.

  10. In Chromeleon, consider updating the Predictive Performance information for the gas filter assembly.

  11. Turn on the gas flow. See Turning On/Off the Detector Gas Flow.