NOTE

For the Dionex DRS 600 in Legacy Mode, as well as the Dionex ERS 500e and Dionex AERS 500 Carbonate, the suppressor voltage is a good indicator of the resistance across the suppressor. Higher voltage may indicate contamination of the suppressor. For more information regarding monitoring the voltage, see Document No. 031841-02 “Removal of Iron Contamination from Electrolytic Suppressors.”

Procedure

  1. Turn off the suppressor power and system pump.
  2. Disconnect the analytical (and guard) column(s) from the injection valve and the suppressor. Refer to the specific analytical column Product Manual for column cleanup procedures.
  3. If you are running in the Auto Suppression External Water Mode, turn off the external water and disconnect the external water line from the suppressor REGEN IN port.
  4. Disconnect the liquid line from the suppressor ELUENT OUT port to the cell at the cell fitting and reconnect it to the REGEN IN port.
  5. If iron is present, then connect a temporary line from the priming block or the low-pressure tee on the isocratic or gradient pump to a container with a solution of 0.2 M oxalic acid. For 4 mm systems pump this solution through the suppressor at 1 – 2 mL/min for 30 minutes. For 2 mm systems pump this solution through the suppressor at 0.25–0.50 mL/min for 30 minutes.
  6. NOTE

    Bypassing internal pump manifolds when temporarily pumping high concentration cleaning solutions significantly reduces the time required to re-equilibrate the system to low concentration eluents.

  7. Perform an extended regeneration, as outlined in Full or extended regeneration.
  8. Reinstall the analytical (and guard) column(s). Begin pumping eluent through the system at the flow rate required for your analysis and equilibrate the system and resume normal operation.

NOTE

Chromeleon 6.5 and later includes a feature to trend various parameters. Trend plotting the suppressor voltage will reveal if there is a build-up of metal contaminants or precipitates in the suppressor. A slow but steady increase in voltage indicates such a contamination build-up